|
1995
|
U. Geiser, J.A. Schlueter,
K.D. Carlson, J.M. Williams, H.H. Wang, W.-K. Kwok, U. Welp, J.A. Fendrich,
J.D. Dudek, C.A. Achenbach, A.S. Komosa, P.M. Keane, D. Naumann, T.
Roy, J.E. Schirber, W.R. Bayless, J. Ren and M.-H. Whangbo
New ET-based organic superconductors with the organometallic
anion [Cu(CF3)4)]-; Synthetic
Metals 70 (1995) 1105-1108. |
R. Miethchen, M.
Hein, D. Naumann and W. Tyrra O-Difluoromethylations
of Monosaccharides by Trifluoromethylzinc Bromide; Liebigs
Ann. 1995, 1717-1719. |
H.
Hau Wang, J.A. Schlueter, U. Geiser, J.M. Williams, D. Naumann und T.
Roy
ESR
Characterization of the Organic Superconducting Salts of the BEDT-TTF
Donor Molecule with the Novel Organometallic Anion [Cu(CF3)4]
[BEDT-TTF = bis(ethylenedithio)tetrathiofulvalene];
Inorg. Chem. 34 (1995) 5552-5557. |
K.
Ludovici, D. Naumann, G. Siegemund, W. Tyrra, H.-G. Varbelow und H.
Wrubel
Neue Syntheseverfahren
für Nitrosoperfluoralkane CnF2n+1NO (n =
1,2,3,6);
Fluorine Chem. 73 (1995) 273-274. |
R. Möckel, W.
Tyrra und D. Naumann Carbenoid
reactions of trifluoromethylelement compounds. Part 2. The reactions
of Cd(CF3)2•2 CH3)CN with cyclic
ethers and thioethers. 113Cd nmr and 19F nmr study of the intermediates;
J. Fluorine Chem. 73 (1995) 229-235. |
W. Tyrra, D. Naumann,
S.V. Pasenok und Yu.L. Yagupolskii Carbenoid
reactions of trifluoromethyl element compounds. Part 4. Reactions of
trifluoromethylzinc bromide with enamines and methylene bases;
J. Fluorine Chem. 70 (1995) 181-185. |
D. Naumann und A.
Meurer Preparation of [NEt4][IF2]
by the reaction of IF with [NEt4]F; J.
Fluorine Chem. 70 (1995) 83-84. |
D. Naumann,
R. Gnann, V. Padelidakis und W. Tyrra Synthesis
and Characterization of (2,6-Difluorophenyl)xenon(II) and Bis(2,6-Difluorophenyl)iodine(III)
Trifluoromethanesulfonates; J. Fluorine
Chem. 72 (1995) 79-82. |
R. Kasemann,
C. Lichenheim, G. Nowicki und D. Naumann Ein
neuer Syntheseweg für Perfluororganoselen- und -tellur-Verbindungen;
Z. anorg. allg. Chem. 621 (1995) 213-217. |
D. Naumann,
R. Gnann, N. Ignat'ev und S. Datsenko Electrochemical
Reduction of Arylxenon Tetrafluoroborates; Z.
anorg. allg. Chem. 621 (1995) 851-853. |
D. Naumann
und M. Kaiser Ein neuer Syntheseweg für
Perfluororganomangan- und -rhenium-Verbindungen; Z.
anorg. allg. Chem. 621 (1995) 812-816. |
J.A.
Schlueter, J.M. Williams, U. Geiser, J.D. Dudek, M.E. Kelly, S.A. Sirchio,
K.D. Carlson, D. Naumann, T. Roy and C.F. Campana Seven
New Organic Superconductors in the System (ET)2M(CF3)4•(Solvent)
(M = Cu, Ag): Effect of Solvent Replacement; Adv.
Mat. 7 (1995) 634-639. |
A. Schlueter,
J.M. Williams, U. Geiser, J.D. Dudek, S.A. Sirchio, M.E. Kelly,
J.S. Gregar, W.H. Kwok, J.A. Fendrich, J.E. Schirber, N.R. Bayless,
D. Naumann and T. Roy Synthesis and Characterization
of Two New Organic Superconductors,
KL- and KH(ET)2 Au(CF3)4•(1,1,2-Trichloroethane)
via Microelectrocrystallization •ET = Bis(ethylene-dithio)tetrathiafulvalene;
J. Chem. Soc., Chem. Commun. 1995, 1311-1312. |
D. Naumann
On fluoroorganotellurium, Iodine and Xenon
derivatives; J. Fluorine Chem. 71
(1995) 179-180. |
|
1996
|
W. Dukat,
F. Gall, Ch. Meyer, D. Mootz, D. Naumann, G. Nowicki und K. Schulz;
Kristallstruktur von CF3TeTeCF3-
Synthese, Charakterisierung und Eigenschaften von CF3TeI
Z. Anorg. Allg. Chem. 622 (1996) 617-621. |
W.
Tyrra und D. Naumann; Trifluormethylzinkbromid
- ein bequem handhabbares Trifluor- und Difluormethylierungsmittel
J. Prakt. Chem. 338 (1996) 283-286 |
J.A.
Schlueter , J.M. Williams, A.M. Kini, U. Geiser, J.D. Dudek, M.E. Kelly,
J.P. Flynn, D. Naumann und T. Roy; New
Directions in the Synthesis and Exploration of Novel Organic Superconductors:
Inverse Isotope Effect in the Organic Superconductor KL-(ET)2-Ag(CF3)4(1-bromo-1,2
dichloroethane)-[ET=bis(ethylenedithio)tetrathiafulvalene];
Physics C 265 (1996) 163-170. |
Wosnitza,
D. Beckmann, S. Wanka, J. Schlueter, J.M. Williams, D. Naumann und T.
Roy; Thermodynamic Properties of the
Organic Superconductor KL(ET)2Ag(CF3)4•TCE;
J. Solid State Commun. 98 (1996)
21-25. |
T.
Lewe, D. Naumann, G. Nowicki, H. Schneider, W. Tyrra, T. Gilles und
K.-F. Tebbe; Synthesen und Eigenschaften
neuer Tris(fluorphenyl)antimon- und -bismut-Verbindungen. Kristallstruktur
von Tris(2,6-difluorphenyl)bismut; Z.
Anorg. Allg. Chem. 622 (1996) 2009-2015. |
H.H.
Wang, M.L. van Zile, U. Geiser, J.A. Schlueter, J. M. Williams, A.M.
Kini, P.P. Sche, P.G. Nixon, R.W. Winter, G.L. Gard, D. Naumann und
T. Roy; 2SF5CH2CF2SO3
and KLþ-(BEDT-TTF)2Cu(CF3)4(DBCE);
1. Proceedings of the International Conference
on Science and Technology of Syntetic Metals, 28.7.-2.8.1996, Snowbird,
Utah, USA;Synthetic Metals. |
E.
Eldridge, Y. Xie, J.A. Schlueter, J.M. Williams, D. Naumann und T. Roy;
Infrared optical properties of the organic superconductor
KL-(BEDT-TTF) Cu(CF3)4×TCE (Tc=4K)
Solid State Commun. 99 (1996) 335-340. |
J.A.
Schlueter, J.M. Williams, U. Geiser, H.H. Wang, A.M. Kini, M.E. Kelly,
J.D. Dudek, D. Naumann und T. Roy; New
organic superconductors in the system (ET)2M(CF3)4
(solvent) (M=Cu, Ag, Au): dramatic effects of organometallic anion and
solvent replacement; Mol.
Cryst. Liq. Cryst. 285 (1996) 43-50. |
J.A.
Schlueter, U. Geiser, H.H. Wang, M.E. Kelly, J.D. Dudek, J.M. Williams,
D. Naumann und T. Roy; Synthesis and
physical properties of a novel, highly tunable family of organic super-conductors:
(ET)2M(CF3)4(1,1,2-trihaloethane)(M=Cu,
Ag, Au); Mol. Cryst. Liq. Cryst. 284
(1996) 195-202. |
K.-F.
Tebbe, T. Gilles, F. Conrad und W. Tyrra Bis(triphenylphosphin)iminium-Tetrakis(pentafluorphenyl)gallat
Acta Cryst. C52 (1996) 1663
- 1666. |
|
1997
|
T.
Lewe, D. Naumann, G. Nowicki, H. Schneider und W. Tyrra;
Eigenschaften und Reaktionen von Tris(2,6-difluorphenyl)bismut(III)
und Tris(2,6-difluor-phenyl)bismut(V)-Verbindungen; Z.
Anorg. Allg. Chem. 623 (1997) 122-128. |
Naumann,
W. Wessel, J. Hahn und W. Tyrra; Darstellung,
NMR-spektroskopische Charakterisierung und Reaktionen von Perfluor-alkylsilber(I)-Verbindungen;
J. Organomet. Chem. 547 (1997)
79-88. |
D.
Naumann, G. Nowicki und K.-J. Sassen;
Synthesen und Eigenschaften von Tris(perfluoralkyl)arsen- und -antimon(III,V)-
Verbindungen Z. Anorg. Allg. Chem. 623
(1997) 1183-1189. |
W.
Tyrra, M. Miczka und D. Naumann; Die
NMR-Spektren von CF3I, CF3IF2 und CF3IF4
Z. Anorg. Allg. Chem. 623 (1997) 1857-1859. |
D.
Naumann, W. Tyrra und T. Lewe; Synthesis
and characterization of new pentafluorophenylbismuth(V) derivatives;
J. Fluorine Chem. 84 (1997)
69-73. |
D.
Naumann, W. Tyrra, R. Gnann, D. Pfolk, T. Gilles und K.F. Tebbe;
The direct synthesis of arylxenon trifluoromethanesulfonates
via electrophilic substitution; Z. Anorg.
Allg. Chem. 623 (1997) 1821-1834. |
J.A.
Schlueter, U. Geiser, H. Hau Wang, M.L. Van Zile, S.B. Fox, J.M. Williams,
A. Laguna, M .Laguna, D. Naumann und Th. Roy; Electrochemical
Synthesis and Crystallization of a Novel Tetraarylaurate Anion: Synthesis,
Structure and Physical Properties of (BEDT-TTF) Au(C6Cl5)4;
Inorg. Chem. 36 (1997) 4265-4269. |
|
1998
|
D.
Naumann und P. Sartori; Martin Schmeißer.
A Brief Biography J. Fluorine Chem.
90 (1998) 195-196 |
J.
Padelidakis, W. Tyrra, F. Conrad und D. Naumann; Synthesis
and Characterization of Cadmiumbis(2,6-difluorobenzoate), Cd[OCO(2,6-F2C6H3)]2,
and Bis(2,6-difluorophenyl)cadmium, Cd(2,6-F2C6H3)2;
J. Fluorine Chem. 91 (1998)
219-220. |
H.
Layeghi, W. Tyrra und D. Naumann; Untersuchungen
zu Synthese und Reaktionen von Fluorphenylquecksilber-Derivaten mit
den Liganden 2-FC6H4, 2,6-F2C6H3
und 2,4,6-F3C6H2; Z.
Anorg. Allg. Chem. 624 (1998) 1601-1610. |
Z.-H.
Choi and W. Tyrra; On the Chemistry of
Fluoroorgano Derivatives of Group 13 Elements. 1. The Reactions of Perfluoroiodoalkanes
and Pentafluoroiodobenzene with Triethylindium - Synthesis and Characterization
of In(C2H5)2(C6F5)•N(C2H5)3
and In(C2H5)2(i-C3F7)•N(C2H5)3
and spectroscopic evidence for bis(3,3,4,4,4-pentafluorobutyl)indium
iodide. Z. Anorg. Allg. Chem. 624
(1998) 2015 - 2020. |
|
1999
|
W.
Tyrra, D. Naumann, N. V. Kirij, A. A. Kolomeitsev und Yu. L. Yagupolskii;
The first alkyl bismuthates, -tris(trifluoromethyl)fluoro-
and tetrakis(trifluoromethyl)-bismuthates; J.
Chem. Soc., Dalton Trans. (1999) 657-658. |
D.
Naumann, Chr. Schorn und W. Tyrra; Synthesen
und Eigenschaften von Bis(perfluoralkyl)zink-Verbindungen;
Z. Anorg. Allg. Chem. 625 (1999) 827-830. |
S.
V. Pasenok, Yu. L. Yagupolskii, W. Tyrra und D. Naumann;
Carbenoid Reactions of Trifluoromethyl Element Compounds.
Part 3. The Reactions of Zn(CF3)Br•2CH3CN
with Phenol, Pentafluorophenol, their Potassium and Ammonium Salts;
Z. Anorg. Allg. Chem. 625 (1999) 831-833. |
S.
V. Pasenok, N. V. Kirij, Yu. L. Yagupolskii, D. Naumann, W. Tyrra und
A. Fitzner; Carbenoid Reactions of Trifluoromethyl
Element Compounds. Part 5. Difluoromethylation of Amines with Zn(CF3)Br•2CH3CN,
Cd(CF3)2•2CH3CN and the System
Bi(CF3)3 / AlCl3 Z.
Anorg. Allg. Chem. 625 (1999) 834-838. |
N.
V. Kirij, S. V. Pasenok, Yu. L.Yagupolskii, A. Fitzner, W. Tyrra und
D. Naumann; Carbenoid Reactions of Trifluoromethyl
Element Compound. Part 6. Syntheses and Characterization of Difluoromethylphosphonium,
Arsonium and Stibonium Compounds from Reactions of Triorganopnicogens
with Zn(CF3)Br•2D and Bi(CF3)3
Fluorine Chem. 94 (1999) 207-212. |
D.
Naumann, N. Maggiarosa, W. Tyrra, N. V. Kirij und Yu. L. Yagupolskii;
[Me3Si(CF3)F]-
und [Me3Si(CF3)2]- - die
reaktiven Zwischenstufen in Fluorid-initiierten Trifluor- Methylierungsreaktionen
mit Me3SiCF3 - eine NMR-Studie; Angew.
Chem. 111 (1999) 2392-2393; Angew. Chem. Int. Ed. Engl. 38
(1999) 2252-2253 |
V.
Padelidakis, W. Tyrra und D. Naumann; Synthesis
and characterization of 2,6-difluorophenyliodine(III) derivatives;
J. Fluorine Chem. 99 (1999) 9-15.
|
T.
Lewe, W. Tyrra und D. Naumann; The reactions
of tris(polyfluorophenyl)bismuth with polyfluorophenyliodine(III) difluoride.
Selective synthesis of bis(polyfluorophenyl)iodine(III) hexafluoroniobates;
J. Fluorine Chem. 99 (1999) 123-125.
|
| Review
J.A. Schlueter, U. Geiser, A.M. Kini, H.H. Wang,
J.M. Williams, D. Naumann, T. Roy, B. Hoge und R. Eujen;
Trifluoromethylmetallate anions as components
of molecular charge transfer salts and superconductors;
Coord. Chem. Rev. 190-192 (1999)
781-810.
|
2000 |
D.
Naumann, W. Tyrra, F. Trinius, W. Wessel und T. Roy; Über
Perfluoralkylsilber(III)-Verbindungen; J.Fluorine
Chem. 101 (2000) 131-135. |
D.
Naumann, T. Roy, B. Caeners, D. Hütten, K.-F. Tebbe und T. Gilles;
Synthesen und Eigenschaften von Perfluorethylkupfer(I)-
und -(III)-Verbindungen:
Cu(C2F5)•D, [Cu(C2F5)2]-
und (C2F5)2CuSC(S)N(C2H5)2;
Z. Anorg. Allg. Chem. 626 (2000)
999-1003. |
N.V.
Kirij, S.V. Pasenok, Yu.L. Yagupolskii, W. Tyrra und D. Naumann;
Bi(CF3)3/Cu(OCOCH3)2
- a new system for the synthesis of 2-trifluoromethylcycloalkan-1-ones,
trifluoromethylanilines and phenyl(trifluoromethyl)sulfane;
J. Fluorine Chem. 106 (2000) 217-221. |
N.
Maggiarosa, D. Naumann und W. Tyrra; Bis(pentafluorphenyl)xenon,
Xe(C6F5)2 - ein homoleptisches Diarylxenon-Derivat;
Angew. Chem. 112 (2000) 4759-4762;
Angew. Chem. Int. Ed. 39 (2000) 4588-4591. |
2001 |
Chr.
Schorn, D. Naumann, H. Scherer und J. Hahn; Concepts
of the NMR structural analysis of perfluoroalkyl groups: characterization
of bis(n- perfluoroalkyl)zinc compounds Zn(CmF2m+1)2•2
THF (m = 4, 6, 7, 8) and Zn(n-C6F13)2•
2 CH3CN; J. Fluorine Chem.
107 (2001) 159-169. |
N.
V. Kirij, S. V. Pasenok, Yu. L. Yagupolskii, D. Naumann und W. Tyrra;
Carbenoid Reactions of Organoelemet
Compounds. VII. Difluorocyclopropanation of olefins and dienes with
the system Bi(CF3)3/AlCl3;
Zh. Org. Khim. (Russ.) 37 (2001)
220-222; Russ. J. Org. Chem. 37 (2001) 207-209. |
W.
Wessel, W. Tyrra und D. Naumann; Synthese
und Eigenschaften von Diethyldithiocarbaminsäureperfluororganylestern,
(C2H5)2NC(S)SRf (Rf
= CF3, C2F5, i-C5F7,
n-C4F9, C6F5);
Z. Anorg. Allg. Chem. 627 (2001)
1264-1268. |
N.
V. Kirij, Yu. L. Yagupolskii, N. V. Petukh, W. Tyrra und D. Naumann;
Trifluoromethylation of heterocumulenes with
trimethyl(trifluoromethyl)silane in the presence of fluoride ions: synthesis
of trifluoroacetamides and trifluorothioacetamides from isocyanates
and isothiocyanates; Tetrahedron Letters
42 (2001) 8181-8183. |
P.
Panne, D. Naumann und B. Hoge; Cyanide
Initiated Perfluoroorganylations with Perfluoroorgano Silicon Compounds;
J. Fluorine Chem. 112 (2001) 283-286. |
N.V.
Kirij, Yu.L. Yagupolskii, N. Maggiarosa, W. Tyrra und D. Naumann;
Tris(trifluoromethyl)tellurate(II), [Te(CF3)3]-
, the dimeric bis(trifluoromethyl)chlorotellurate(II), [(CF3)2TeCl]22-,
and bis(trifluoromethyl)iodate(I), [I(CF3)2]-:
the first hypervalent alkyl [10-Te-3] and [10-Te-4] species and a novel
[10-I-2] compound: J. Fluorine Chem.
112 (2001) 213-218. |
| Review |
D.
Naumann; On Perfluoroalkyl Tellurium
Compounds; Phosphorus, Sulfur and Silicon
171 (2001) 113-133. |
| Patent |
P.
Neu, F. Schucht, W. Tyrra und D. Naumann; Quantitative
Bestimmung des Xenongehaltes in Flüssigkeiten mit Hilfe der NMR-Spektroskopie
(Messer-Griesheim) Offenlegung DE 19942278
A1; 12.04.2001; Intern. Veröffentlichung WO 01/18534 A1; 15.03.2001. |
2002
|
H.
Bock, D. Hinz-Hübner, U. Ruschewitz und D. Naumann;
Struktur von Bis(pentafluorphenyl)xenon, Xe(C6F5)2;
Angew. Chem. 114 (2002) 465-467;
Angew. Chem. Int. Ed. 41 (2002) 448-450. |
| Yu.L.
Yagupolskii, W. Tyrra, R. Gnann, N. Maggiarosa und D. Naumann;
2,6-Difluorphenylxenon(II)bis(fluorsulfanyl)amid,
-bis(trifluormethylsulfonyl)amid, -tris(fluor-
sulfonyl)methanid und -bis(trifluormethylsulfonyl)methanid;
J. Fluorine Chem. 113 (2002)
143-146. |
D.
Naumann, W. Tyrra, R. Herrmann, I. Pantenburg und M.S. Wickleder;
Syntheses and Properties of Tetrakis(pentafluorphenyl)tellurium,
Te(C6F5)4
and Related
Compounds. Single Crystal Structures of Tris(pentafluorophenyl)tellurium
Bromide, Te(C6F5)3Br,
Tris(pentafluorophenyl)tellurium Trifluoromethanesulfonate, [Te(C6F5)3][OSO2CF3],
and Bis- (pentafluorophenyl)tellurium Oxide, Te(C6F5)2O;
Z. Anorg. Allg. Chem. 628 (2002)
833-842. |
Yu.L.
Yagupolskii, N.V. Kirij, A.V. Shevchenko, W. Tyrra und D. Naumann;
Perfluoroalkylation of heterocumulenes with trimethyl(perfluoroalkyl)silanes
in the presence of fluoride ions: synthesis of perfluoroalkane sulfinyl
amides from N-organyl sulfinyl amines; Tetrahedron
Lett. 43 (2002) 3029-3031. |
| Review |
| W.
Tyrra und D. Naumann;
Organoxenon Compounds;
in G. Meyer, D. Naumann und L. Wesemann (Eds.),
Inorganic Chemistry Highlights, Wiley- VCH, Weinheim, 2002; S. 297-316. |
2003 |
W.
Tyrra, D. Naumann, B. Hoge und Yu.L. Yagupolskii; A
new synthesis of trifluoromethanethiolates – characterization
and properties of tetramethylammonium, cesium and di(benzo-15-crown-5)cesium
trifluoromethanethiolates; J. Fluorine
Chem. 119 (2003) 101-107. |
W.
Tyrra, D. Naumann und I. Pantenburg; Synthesis
and crystal structures of bis(4-dimethylaminopyridine) group 12 trifluoroacetates
- M(OCOCF3)2 •2DMAP (M = Zn, Cd, Hg);
J. Fluorine. Chem. 120 (2003)
13-19. |
B.
Hoge, D. Naumann, H. Pohl und J. Shamir Vibrational
spectra and structures of fluoroalkyl and fluoroaryl compounds of tellurium:
Te2(CF3)2, Te2(C6F5)2
and Te(C6F5)2; J.
Raman Spectr. 34 (2003) 33-39. |
W. Tyrra, D. Naumann, H. Pohl und I. Pantenburg
Trifluoromethylselenate(0), [SeCF3]¯, and
Trifluoromethyltellerate(0), [TeCF3]¯ - Crystalline Products
of the Reduction of the Bis(trifluoromethyl)dichelkogen
Compounds, E2(CF3)2 (E = Se, Te), with Tetrakis(dimethylamino)ethene
(TDAE);
Z. Anorg. Allg. Chem. 629 (2003)
1039-104 |
W. Tyrra, D. Naumann und Yu.L. Yagupolskii; Stable
trifluoromethylselenates(0); [A]SeCF3 – synthesis, characterizations
and properties; J. Fluorine Chem. 123
(2003) 183-187. |
F. Schulz, I. Pantenburg und D. Naumann; Synthesen
und Strukturen von Perfluororganohalogenomercuraten [Hd(Rf)X]¯
(Rf = CF3, C6F5; X = Br, I); Z. Anorg.
Allg. Chem. 629 (2003) 2312-2616. |
2004 |
D. Naumann, F. Schulz, I. Pantenburg und W. Tyrra;
Strukturen von Bis(trifluormethyl)halogeno- und
–thiocyanato-mercuraten, [Hg(CF3)2X]¯ (X = Br, I, SCN), und
ein Vergleich der Strukturparameter der CF3-Gruppen;
Z. Anorg. Allg. Chem. 630 (2004)
529-534. |
H.
Schmidt, H. Scherer, W. Tyrra, J. Hahn und D. Naumann;
Alkynylxenon(II) Fluorides;
Inorg. Chem. 43 (2004) 1837-1839. |
D.
Naumann, N.V. Kirij, N. Maggiarosa, W. Tyrra, Yu.L. Yagupolskii und
M. Wickleder;
Synthesen und Charakterisierungen der ersten Tris-
und Tetrakis(trifluormethyl)palladate(II) und
– platinate(II), [M(CF3)3(PPh3)]¯ und [M(CF3)4]2– (M
= Pd, Pt);
Z. Anorg. Allg. Chem. 630 (2004)
746-751. |
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